TY - JOUR
T1 - A new method of fabrication of TiC by employing pyrolytic carbon black and titanium
AU - Jianxin, Wang
AU - Gao Dongshan, Ni Yaru
AU - Chunhua, Lu
AU - Zhanggang, Fang
AU - Zhongzi, Xu
PY - 2014/7
Y1 - 2014/7
N2 - A new method to synthesize titanium carbide (TiC) from polysiloxanes and titanium (Ti) by employing an in situ reaction is presented. The factors, such as, the annealing temperature and Ti particle size, were found to play a significant effect on the phase composition, structure, thermal behavior, and textural morphology of as-prepared TiC. Moreover, the relative intensity ratio (RIR) method was applied to evaluate the phase purity of TiC. Results demonstrated that the phase purity of the TiC prepared at 1400 °C for 2 h under the argon atmosphere is approximately up to 100%, confirming the feasibility of the presented new method.
AB - A new method to synthesize titanium carbide (TiC) from polysiloxanes and titanium (Ti) by employing an in situ reaction is presented. The factors, such as, the annealing temperature and Ti particle size, were found to play a significant effect on the phase composition, structure, thermal behavior, and textural morphology of as-prepared TiC. Moreover, the relative intensity ratio (RIR) method was applied to evaluate the phase purity of TiC. Results demonstrated that the phase purity of the TiC prepared at 1400 °C for 2 h under the argon atmosphere is approximately up to 100%, confirming the feasibility of the presented new method.
KW - Annealing
KW - In situ reaction
KW - RIR method
KW - Titanium carbide
UR - http://www.scopus.com/inward/record.url?scp=84899827325&partnerID=8YFLogxK
U2 - 10.1016/j.ijrmhm.2014.04.002
DO - 10.1016/j.ijrmhm.2014.04.002
M3 - 文章
AN - SCOPUS:84899827325
SN - 0263-4368
VL - 45
SP - 137
EP - 140
JO - International Journal of Refractory Metals and Hard Materials
JF - International Journal of Refractory Metals and Hard Materials
ER -