CSC-P(AM-AA)重金属捕集絮凝剂的光谱表征及其对重金属去除研究

Xue Feng Xiao; Yong Jun Sun; Hao Shen; Wen Qaun Sun; Huai Li Zheng; Yan Hua Xu; Cheng Yu Zhu

doi:10.3964/j.issn.1000-0593(2018)06-1809-05

CSC-P(AM-AA)重金属捕集絮凝剂的光谱表征及其对重金属去除研究

Translated title of the contribution: Spectral Characterizations of CSC-P(AM-AA) with Function of Trapping Heavy Metals and Its Removal Efficiency of Cu²⁺

Xue Feng Xiao, Yong Jun Sun, Hao Shen, Wen Qaun Sun, Huai Li Zheng, Yan Hua Xu, Cheng Yu Zhu

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

In this paper, the graft terpolymer, which is called Chitosan-based heavy metal capture flocculant CSC-P(AM-AA), of carboxymethyl chitosan (CSC) and acrylamide (AM) and acrylic acid (AA) were successfully prepared by photopolymerization. In order to demonstrate the successful preparation and characterization of the graft copolymer, the IR spectra, XRD, TG-DSC, and scanning electron microscopy (SEM) were used to characterize the product polymer. The results showed that the graft copolymer of CSC-P (AM-AA) was successfully prepared, and the graft copolymer had good soluble ability. In addition, P (AM-AA) had a structural characteristics that were significantly different from those of P(AM-AA), due to the graft polymerization of carboxymethyl chitosan. The flocculation results showed that CSC-P(AM-AA) had good heavy metal removal performance. At pH 8, dosage of 8 mg•L^-1, and rotation speed of 150 r•min^-1, the optimal removal rate of Cu²⁺ by CSC-P(AM-AA) was 87.0%.

Translated title of the contribution	Spectral Characterizations of CSC-P(AM-AA) with Function of Trapping Heavy Metals and Its Removal Efficiency of Cu²⁺
Original language	Chinese (Traditional)
Pages (from-to)	1809-1813
Number of pages	5
Journal	Guang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysis
Volume	38
Issue number	6
DOIs	https://doi.org/10.3964/j.issn.1000-0593(2018)06-1809-05
State	Published - 1 Jun 2018

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@article{44b33d3a16ce479bbe37254bf9220010,

title = "CSC-P(AM-AA)重金属捕集絮凝剂的光谱表征及其对重金属去除研究",

abstract = "In this paper, the graft terpolymer, which is called Chitosan-based heavy metal capture flocculant CSC-P(AM-AA), of carboxymethyl chitosan (CSC) and acrylamide (AM) and acrylic acid (AA) were successfully prepared by photopolymerization. In order to demonstrate the successful preparation and characterization of the graft copolymer, the IR spectra, XRD, TG-DSC, and scanning electron microscopy (SEM) were used to characterize the product polymer. The results showed that the graft copolymer of CSC-P (AM-AA) was successfully prepared, and the graft copolymer had good soluble ability. In addition, P (AM-AA) had a structural characteristics that were significantly different from those of P(AM-AA), due to the graft polymerization of carboxymethyl chitosan. The flocculation results showed that CSC-P(AM-AA) had good heavy metal removal performance. At pH 8, dosage of 8 mg•L-1, and rotation speed of 150 r•min-1, the optimal removal rate of Cu2+ by CSC-P(AM-AA) was 87.0%.",

keywords = "Chitosan, Flocculants, Graft copolymerization, Heavy metals, Spectral characterizations",

author = "Xiao, {Xue Feng} and Sun, {Yong Jun} and Hao Shen and Sun, {Wen Qaun} and Zheng, {Huai Li} and Xu, {Yan Hua} and Zhu, {Cheng Yu}",

year = "2018",

month = jun,

day = "1",

doi = "10.3964/j.issn.1000-0593(2018)06-1809-05",

language = "繁体中文",

volume = "38",

pages = "1809--1813",

journal = "Guang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysis",

issn = "1000-0593",

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number = "6",

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T1 - CSC-P(AM-AA)重金属捕集絮凝剂的光谱表征及其对重金属去除研究

AU - Xiao, Xue Feng

AU - Sun, Yong Jun

AU - Shen, Hao

AU - Sun, Wen Qaun

AU - Zheng, Huai Li

AU - Xu, Yan Hua

AU - Zhu, Cheng Yu

PY - 2018/6/1

Y1 - 2018/6/1

N2 - In this paper, the graft terpolymer, which is called Chitosan-based heavy metal capture flocculant CSC-P(AM-AA), of carboxymethyl chitosan (CSC) and acrylamide (AM) and acrylic acid (AA) were successfully prepared by photopolymerization. In order to demonstrate the successful preparation and characterization of the graft copolymer, the IR spectra, XRD, TG-DSC, and scanning electron microscopy (SEM) were used to characterize the product polymer. The results showed that the graft copolymer of CSC-P (AM-AA) was successfully prepared, and the graft copolymer had good soluble ability. In addition, P (AM-AA) had a structural characteristics that were significantly different from those of P(AM-AA), due to the graft polymerization of carboxymethyl chitosan. The flocculation results showed that CSC-P(AM-AA) had good heavy metal removal performance. At pH 8, dosage of 8 mg•L-1, and rotation speed of 150 r•min-1, the optimal removal rate of Cu2+ by CSC-P(AM-AA) was 87.0%.

AB - In this paper, the graft terpolymer, which is called Chitosan-based heavy metal capture flocculant CSC-P(AM-AA), of carboxymethyl chitosan (CSC) and acrylamide (AM) and acrylic acid (AA) were successfully prepared by photopolymerization. In order to demonstrate the successful preparation and characterization of the graft copolymer, the IR spectra, XRD, TG-DSC, and scanning electron microscopy (SEM) were used to characterize the product polymer. The results showed that the graft copolymer of CSC-P (AM-AA) was successfully prepared, and the graft copolymer had good soluble ability. In addition, P (AM-AA) had a structural characteristics that were significantly different from those of P(AM-AA), due to the graft polymerization of carboxymethyl chitosan. The flocculation results showed that CSC-P(AM-AA) had good heavy metal removal performance. At pH 8, dosage of 8 mg•L-1, and rotation speed of 150 r•min-1, the optimal removal rate of Cu2+ by CSC-P(AM-AA) was 87.0%.

KW - Chitosan

KW - Flocculants

KW - Graft copolymerization

KW - Heavy metals

KW - Spectral characterizations

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DO - 10.3964/j.issn.1000-0593(2018)06-1809-05

M3 - 文章

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CSC-P(AM-AA)重金属捕集絮凝剂的光谱表征及其对重金属去除研究

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