Fabrication of chitosan-mesoporous silica SBA-15 nanocomposites via functional ionic liquid as the bridging agent for PPL immobilization

Xinran Xiang; Song Ding; Hongbo Suo; Chao Xu; Zhen Gao; Yi Hu

doi:10.1016/j.carbpol.2017.11.031

Fabrication of chitosan-mesoporous silica SBA-15 nanocomposites via functional ionic liquid as the bridging agent for PPL immobilization

Xinran Xiang, Song Ding, Hongbo Suo, Chao Xu, Zhen Gao, Yi Hu

Nanjing Tech University

Research output: Contribution to journal › Article › peer-review

53 Scopus citations

Abstract

A nanocomposite (SBA-CIL-CS) which was combined mesoporous silica SBA-15 material with chitosan via ionic liquid as the bridging agent was successfully fabricated. The morphology and structure of the nanocomposite were characterized in detail with transmission electron microscope, fourier transform infrared spectroscopy, thermogravimetric analysis and nitrogen adsorption–desorption techniques. SBA-CIL-CS was investigated as an efficient support for immobilization of porcine pancreas lipase (PPL) and possessed high immobilization efficiency. The properties of immobilized enzyme (SBA-CIL-CS-PPL) such as activity, stability and reusability have been significantly improved, and a preferable pH and temperature tolerance were obtained as well. Results demonstrated the inorganic-organic nanocomposite could be used as an ideal support for enzyme immobilization.

Original language	English
Pages (from-to)	245-253
Number of pages	9
Journal	Carbohydrate Polymers
Volume	182
DOIs	https://doi.org/10.1016/j.carbpol.2017.11.031
State	Published - 15 Feb 2018

Keywords

Chitosan
Enzyme immobilization
Ionic liquid
Mesoporous material
Nanocomposite

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10.1016/j.carbpol.2017.11.031

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title = "Fabrication of chitosan-mesoporous silica SBA-15 nanocomposites via functional ionic liquid as the bridging agent for PPL immobilization",

abstract = "A nanocomposite (SBA-CIL-CS) which was combined mesoporous silica SBA-15 material with chitosan via ionic liquid as the bridging agent was successfully fabricated. The morphology and structure of the nanocomposite were characterized in detail with transmission electron microscope, fourier transform infrared spectroscopy, thermogravimetric analysis and nitrogen adsorption–desorption techniques. SBA-CIL-CS was investigated as an efficient support for immobilization of porcine pancreas lipase (PPL) and possessed high immobilization efficiency. The properties of immobilized enzyme (SBA-CIL-CS-PPL) such as activity, stability and reusability have been significantly improved, and a preferable pH and temperature tolerance were obtained as well. Results demonstrated the inorganic-organic nanocomposite could be used as an ideal support for enzyme immobilization.",

keywords = "Chitosan, Enzyme immobilization, Ionic liquid, Mesoporous material, Nanocomposite",

author = "Xinran Xiang and Song Ding and Hongbo Suo and Chao Xu and Zhen Gao and Yi Hu",

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doi = "10.1016/j.carbpol.2017.11.031",

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T1 - Fabrication of chitosan-mesoporous silica SBA-15 nanocomposites via functional ionic liquid as the bridging agent for PPL immobilization

AU - Xiang, Xinran

AU - Ding, Song

AU - Suo, Hongbo

AU - Xu, Chao

AU - Gao, Zhen

AU - Hu, Yi

PY - 2018/2/15

Y1 - 2018/2/15

N2 - A nanocomposite (SBA-CIL-CS) which was combined mesoporous silica SBA-15 material with chitosan via ionic liquid as the bridging agent was successfully fabricated. The morphology and structure of the nanocomposite were characterized in detail with transmission electron microscope, fourier transform infrared spectroscopy, thermogravimetric analysis and nitrogen adsorption–desorption techniques. SBA-CIL-CS was investigated as an efficient support for immobilization of porcine pancreas lipase (PPL) and possessed high immobilization efficiency. The properties of immobilized enzyme (SBA-CIL-CS-PPL) such as activity, stability and reusability have been significantly improved, and a preferable pH and temperature tolerance were obtained as well. Results demonstrated the inorganic-organic nanocomposite could be used as an ideal support for enzyme immobilization.

AB - A nanocomposite (SBA-CIL-CS) which was combined mesoporous silica SBA-15 material with chitosan via ionic liquid as the bridging agent was successfully fabricated. The morphology and structure of the nanocomposite were characterized in detail with transmission electron microscope, fourier transform infrared spectroscopy, thermogravimetric analysis and nitrogen adsorption–desorption techniques. SBA-CIL-CS was investigated as an efficient support for immobilization of porcine pancreas lipase (PPL) and possessed high immobilization efficiency. The properties of immobilized enzyme (SBA-CIL-CS-PPL) such as activity, stability and reusability have been significantly improved, and a preferable pH and temperature tolerance were obtained as well. Results demonstrated the inorganic-organic nanocomposite could be used as an ideal support for enzyme immobilization.

KW - Chitosan

KW - Enzyme immobilization

KW - Ionic liquid

KW - Mesoporous material

KW - Nanocomposite

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U2 - 10.1016/j.carbpol.2017.11.031

DO - 10.1016/j.carbpol.2017.11.031

M3 - 文章

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AN - SCOPUS:85033366170

SN - 0144-8617

VL - 182

SP - 245

EP - 253

JO - Carbohydrate Polymers

JF - Carbohydrate Polymers

ER -

Fabrication of chitosan-mesoporous silica SBA-15 nanocomposites via functional ionic liquid as the bridging agent for PPL immobilization

Abstract

Keywords

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