GC-MS analysis of impurities in p-phenetidine sample

Rong Sun; Cheng Yao; Jie Chen; Yabing Feng

GC-MS analysis of impurities in p-phenetidine sample

Rong Sun, Cheng Yao, Jie Chen, Yabing Feng

School of Chemistry and Moleculai Engineering

Research output: Contribution to journal › Article › peer-review

Abstract

A GC-MS method was established to analyze the impurities of p-phenetidine sample. The structure of the impurities were identified to be N-methyl-4-ethoxybenzenamine, N-ethyl-4-ethoxy-benzenamine, N-methoxy-4-ethoxybenzenamine, N-(4-ethoxybenzenamine) phenyl-1, 4-diamine and N ¹-ethoxy-N ⁴-Cethoxybenzenamine) phenyl-1,4-diamine by MS, and indicated that the impurities mainly resulted from the reaction conditions and the solvent methanol. This GC-MS method is very useful for the later research.

Original language	English
Pages (from-to)	69-71
Number of pages	3
Journal	Speciality Petrochemicals
Volume	27
Issue number	6
State	Published - Nov 2010

Keywords

Analysis of impuritie
GC/MS
p-phenetidine

Cite this

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title = "GC-MS analysis of impurities in p-phenetidine sample",

abstract = "A GC-MS method was established to analyze the impurities of p-phenetidine sample. The structure of the impurities were identified to be N-methyl-4-ethoxybenzenamine, N-ethyl-4-ethoxy-benzenamine, N-methoxy-4-ethoxybenzenamine, N-(4-ethoxybenzenamine) phenyl-1, 4-diamine and N 1-ethoxy-N 4-Cethoxybenzenamine) phenyl-1,4-diamine by MS, and indicated that the impurities mainly resulted from the reaction conditions and the solvent methanol. This GC-MS method is very useful for the later research.",

keywords = "Analysis of impuritie, GC/MS, p-phenetidine",

author = "Rong Sun and Cheng Yao and Jie Chen and Yabing Feng",

year = "2010",

month = nov,

language = "英语",

volume = "27",

pages = "69--71",

journal = "Speciality Petrochemicals",

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TY - JOUR

T1 - GC-MS analysis of impurities in p-phenetidine sample

AU - Sun, Rong

AU - Yao, Cheng

AU - Chen, Jie

AU - Feng, Yabing

PY - 2010/11

Y1 - 2010/11

N2 - A GC-MS method was established to analyze the impurities of p-phenetidine sample. The structure of the impurities were identified to be N-methyl-4-ethoxybenzenamine, N-ethyl-4-ethoxy-benzenamine, N-methoxy-4-ethoxybenzenamine, N-(4-ethoxybenzenamine) phenyl-1, 4-diamine and N 1-ethoxy-N 4-Cethoxybenzenamine) phenyl-1,4-diamine by MS, and indicated that the impurities mainly resulted from the reaction conditions and the solvent methanol. This GC-MS method is very useful for the later research.

AB - A GC-MS method was established to analyze the impurities of p-phenetidine sample. The structure of the impurities were identified to be N-methyl-4-ethoxybenzenamine, N-ethyl-4-ethoxy-benzenamine, N-methoxy-4-ethoxybenzenamine, N-(4-ethoxybenzenamine) phenyl-1, 4-diamine and N 1-ethoxy-N 4-Cethoxybenzenamine) phenyl-1,4-diamine by MS, and indicated that the impurities mainly resulted from the reaction conditions and the solvent methanol. This GC-MS method is very useful for the later research.

KW - Analysis of impuritie

KW - GC/MS

KW - p-phenetidine

UR - http://www.scopus.com/inward/record.url?scp=84861518904&partnerID=8YFLogxK

M3 - 文章

AN - SCOPUS:84861518904

SN - 1003-9384

VL - 27

SP - 69

EP - 71

JO - Speciality Petrochemicals

JF - Speciality Petrochemicals

IS - 6

ER -

GC-MS analysis of impurities in p-phenetidine sample

Abstract

Keywords

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