Abstract
The electron emission materials-aluminates have been synthesized by solid-phase reaction and chemistry liquid-phase co-precipitation. The results of XRD and TG-DSC indicate that the optimal synthesis temperature is 1100°C, 150° lower than solid-phase reaction, by chemistry co-precipitation with the crystal phase of Ba5CaAl4O12. The impulse emission current density is 25.3865 A/cm2, and the average evaporation velocity Vevap is 5.04 ×l0-8 (g·cm-2)·s-1. So the aluminates synthesized by chemistry liquid-phase co-precipitation can satisfy the requirement of Ba-W cathodes.
Original language | English |
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Pages (from-to) | 2057-2060 |
Number of pages | 4 |
Journal | Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering |
Volume | 36 |
Issue number | 11 |
State | Published - Nov 2007 |
Keywords
- Aluminate
- Chemistry liquid-phase co-precipitation
- Emission current density
- Impregnated cathode