One-dimensional BiPO4 nanorods and two-dimensional BiOCl lamellae: Fast low-temperature sonochemical synthesis, characterization, and growth mechanism

Jun Geng; Wen Hua Hou; Yi Nong Lv; Jun Jie Zhu; Hong Yuan Chen

doi:10.1021/ic050674g

One-dimensional BiPO₄ nanorods and two-dimensional BiOCl lamellae: Fast low-temperature sonochemical synthesis, characterization, and growth mechanism

Jun Geng, Wen Hua Hou, Yi Nong Lv, Jun Jie Zhu, Hong Yuan Chen

College of Materials Science and Engineering

Research output: Contribution to journal › Article › peer-review

197 Scopus citations

Abstract

Regular BiPO₄ nanorods, for the first time, and BiOCl lamellae have been successfully synthesized via a facile sonochemical method in a surfactant/ligand-free system under ambient air. The as-prepared products are characterized by XRD, TEM, SAED, FE-SEM, HRTEM, and Raman spectroscopy. The effects of pH and ultrasound irradiation on the phase and morphology of the products are studied and the sonochemical formation mechanisms of 1D and 2D structures are discussed. TEM data from samples made after different reaction times suggest an ultrasound-induced nucleation and an oriented-attachment growth mechanism.

Original language	English
Pages (from-to)	8503-8509
Number of pages	7
Journal	Inorganic Chemistry
Volume	44
Issue number	23
DOIs	https://doi.org/10.1021/ic050674g
State	Published - 14 Nov 2005

Access to Document

10.1021/ic050674g

Cite this

@article{d1d22e4db9814ee2a9a83f45cc2e1a87,

title = "One-dimensional BiPO4 nanorods and two-dimensional BiOCl lamellae: Fast low-temperature sonochemical synthesis, characterization, and growth mechanism",

abstract = "Regular BiPO4 nanorods, for the first time, and BiOCl lamellae have been successfully synthesized via a facile sonochemical method in a surfactant/ligand-free system under ambient air. The as-prepared products are characterized by XRD, TEM, SAED, FE-SEM, HRTEM, and Raman spectroscopy. The effects of pH and ultrasound irradiation on the phase and morphology of the products are studied and the sonochemical formation mechanisms of 1D and 2D structures are discussed. TEM data from samples made after different reaction times suggest an ultrasound-induced nucleation and an oriented-attachment growth mechanism.",

author = "Jun Geng and Hou, {Wen Hua} and Lv, {Yi Nong} and Zhu, {Jun Jie} and Chen, {Hong Yuan}",

year = "2005",

month = nov,

day = "14",

doi = "10.1021/ic050674g",

language = "英语",

volume = "44",

pages = "8503--8509",

journal = "Inorganic Chemistry",

issn = "0020-1669",

publisher = "American Chemical Society",

number = "23",

}

TY - JOUR

T1 - One-dimensional BiPO4 nanorods and two-dimensional BiOCl lamellae

T2 - Fast low-temperature sonochemical synthesis, characterization, and growth mechanism

AU - Geng, Jun

AU - Hou, Wen Hua

AU - Lv, Yi Nong

AU - Zhu, Jun Jie

AU - Chen, Hong Yuan

PY - 2005/11/14

Y1 - 2005/11/14

N2 - Regular BiPO4 nanorods, for the first time, and BiOCl lamellae have been successfully synthesized via a facile sonochemical method in a surfactant/ligand-free system under ambient air. The as-prepared products are characterized by XRD, TEM, SAED, FE-SEM, HRTEM, and Raman spectroscopy. The effects of pH and ultrasound irradiation on the phase and morphology of the products are studied and the sonochemical formation mechanisms of 1D and 2D structures are discussed. TEM data from samples made after different reaction times suggest an ultrasound-induced nucleation and an oriented-attachment growth mechanism.

AB - Regular BiPO4 nanorods, for the first time, and BiOCl lamellae have been successfully synthesized via a facile sonochemical method in a surfactant/ligand-free system under ambient air. The as-prepared products are characterized by XRD, TEM, SAED, FE-SEM, HRTEM, and Raman spectroscopy. The effects of pH and ultrasound irradiation on the phase and morphology of the products are studied and the sonochemical formation mechanisms of 1D and 2D structures are discussed. TEM data from samples made after different reaction times suggest an ultrasound-induced nucleation and an oriented-attachment growth mechanism.

UR - http://www.scopus.com/inward/record.url?scp=28244478015&partnerID=8YFLogxK

U2 - 10.1021/ic050674g

DO - 10.1021/ic050674g

M3 - 文章

AN - SCOPUS:28244478015

SN - 0020-1669

VL - 44

SP - 8503

EP - 8509

JO - Inorganic Chemistry

JF - Inorganic Chemistry

IS - 23

ER -

One-dimensional BiPO₄ nanorods and two-dimensional BiOCl lamellae: Fast low-temperature sonochemical synthesis, characterization, and growth mechanism

Abstract

Access to Document

Other files and links

Fingerprint

Cite this