Sol-Gel process for the preparation of ultrafine PbTiO3 powders

Qitu Zhang; Zhiql Zhang; Dawei Shen; Wranrong Xue; Hui Wang; Meiyu Zao

doi:10.1109/ISAF.1992.300568

Sol-Gel process for the preparation of ultrafine PbTiO₃ powders

Qitu Zhang, Zhiql Zhang, Dawei Shen, Wranrong Xue, Hui Wang, Meiyu Zao

College of Materials Science and Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Tetrabutyl titanate and lead acetate are used as the precursors to prepare ultrafine lead titanate (PbTiO₃) powders through the sol-gel process. It is shown that powders with high purity concentration (99.67 wt.%), small particle size (average particle size 0.1 mu m), and narrow size distribution can be obtained. The sol-gel-derived gel was highly crystallized after heat treatment at 400 degrees C for 2 h. It is also found that Pb(CH₃CO₂)₂ can be effectively dehydrated at 190 degrees C.

Original language	English
Title of host publication	ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics
Editors	Ahmad Safari, Michael Liu, Angus Kingon, Gene Haertling
Publisher	Institute of Electrical and Electronics Engineers Inc.
Pages	551-553
Number of pages	3
ISBN (Electronic)	0780304659, 9780780304659
DOIs	https://doi.org/10.1109/ISAF.1992.300568
State	Published - 1992
Event	8th IEEE International Symposium on Applications of Ferroelectrics, ISAF 1992 - Greenville, United States Duration: 30 Aug 1992 → 2 Sep 1992

Publication series

Name	ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics

Conference

Conference	8th IEEE International Symposium on Applications of Ferroelectrics, ISAF 1992
Country/Territory	United States
City	Greenville
Period	30/08/92 → 2/09/92

Access to Document

10.1109/ISAF.1992.300568

Cite this

Zhang, Q., Zhang, Z., Shen, D., Xue, W., Wang, H., & Zao, M. (1992). Sol-Gel process for the preparation of ultrafine PbTiO₃ powders. In A. Safari, M. Liu, A. Kingon, & G. Haertling (Eds.), ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics (pp. 551-553). Article 300568 (ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics). Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/ISAF.1992.300568

Zhang, Qitu ; Zhang, Zhiql ; Shen, Dawei et al. / Sol-Gel process for the preparation of ultrafine PbTiO₃ powders. ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics. editor / Ahmad Safari ; Michael Liu ; Angus Kingon ; Gene Haertling. Institute of Electrical and Electronics Engineers Inc., 1992. pp. 551-553 (ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics).

@inproceedings{d012add982634c1e868c611c24f726a1,

title = "Sol-Gel process for the preparation of ultrafine PbTiO3 powders",

abstract = "Tetrabutyl titanate and lead acetate are used as the precursors to prepare ultrafine lead titanate (PbTiO3) powders through the sol-gel process. It is shown that powders with high purity concentration (99.67 wt.%), small particle size (average particle size 0.1 mu m), and narrow size distribution can be obtained. The sol-gel-derived gel was highly crystallized after heat treatment at 400 degrees C for 2 h. It is also found that Pb(CH3CO2)2 can be effectively dehydrated at 190 degrees C.",

author = "Qitu Zhang and Zhiql Zhang and Dawei Shen and Wranrong Xue and Hui Wang and Meiyu Zao",

note = "Publisher Copyright: {\textcopyright} 1992 IEEE.; 8th IEEE International Symposium on Applications of Ferroelectrics, ISAF 1992 ; Conference date: 30-08-1992 Through 02-09-1992",

year = "1992",

doi = "10.1109/ISAF.1992.300568",

language = "英语",

series = "ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics",

publisher = "Institute of Electrical and Electronics Engineers Inc.",

pages = "551--553",

editor = "Ahmad Safari and Michael Liu and Angus Kingon and Gene Haertling",

booktitle = "ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics",

address = "美国",

}

Zhang, Q, Zhang, Z, Shen, D, Xue, W, Wang, H & Zao, M 1992, Sol-Gel process for the preparation of ultrafine PbTiO₃ powders. in A Safari, M Liu, A Kingon & G Haertling (eds), ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics., 300568, ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics, Institute of Electrical and Electronics Engineers Inc., pp. 551-553, 8th IEEE International Symposium on Applications of Ferroelectrics, ISAF 1992, Greenville, United States, 30/08/92. https://doi.org/10.1109/ISAF.1992.300568

Sol-Gel process for the preparation of ultrafine PbTiO₃ powders. / Zhang, Qitu; Zhang, Zhiql; Shen, Dawei et al.
ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics. ed. / Ahmad Safari; Michael Liu; Angus Kingon; Gene Haertling. Institute of Electrical and Electronics Engineers Inc., 1992. p. 551-553 300568 (ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Sol-Gel process for the preparation of ultrafine PbTiO3 powders

AU - Zhang, Qitu

AU - Zhang, Zhiql

AU - Shen, Dawei

AU - Xue, Wranrong

AU - Wang, Hui

AU - Zao, Meiyu

PY - 1992

Y1 - 1992

N2 - Tetrabutyl titanate and lead acetate are used as the precursors to prepare ultrafine lead titanate (PbTiO3) powders through the sol-gel process. It is shown that powders with high purity concentration (99.67 wt.%), small particle size (average particle size 0.1 mu m), and narrow size distribution can be obtained. The sol-gel-derived gel was highly crystallized after heat treatment at 400 degrees C for 2 h. It is also found that Pb(CH3CO2)2 can be effectively dehydrated at 190 degrees C.

AB - Tetrabutyl titanate and lead acetate are used as the precursors to prepare ultrafine lead titanate (PbTiO3) powders through the sol-gel process. It is shown that powders with high purity concentration (99.67 wt.%), small particle size (average particle size 0.1 mu m), and narrow size distribution can be obtained. The sol-gel-derived gel was highly crystallized after heat treatment at 400 degrees C for 2 h. It is also found that Pb(CH3CO2)2 can be effectively dehydrated at 190 degrees C.

UR - http://www.scopus.com/inward/record.url?scp=85067443792&partnerID=8YFLogxK

U2 - 10.1109/ISAF.1992.300568

DO - 10.1109/ISAF.1992.300568

M3 - 会议稿件

AN - SCOPUS:85067443792

T3 - ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics

SP - 551

EP - 553

BT - ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics

A2 - Safari, Ahmad

A2 - Liu, Michael

A2 - Kingon, Angus

A2 - Haertling, Gene

PB - Institute of Electrical and Electronics Engineers Inc.

T2 - 8th IEEE International Symposium on Applications of Ferroelectrics, ISAF 1992

Y2 - 30 August 1992 through 2 September 1992

ER -

Zhang Q, Zhang Z, Shen D, Xue W, Wang H, Zao M. Sol-Gel process for the preparation of ultrafine PbTiO₃ powders. In Safari A, Liu M, Kingon A, Haertling G, editors, ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics. Institute of Electrical and Electronics Engineers Inc. 1992. p. 551-553. 300568. (ISAF 1992 - Proceedings of the 8th IEEE International Symposium on Applications of Ferroelectrics). doi: 10.1109/ISAF.1992.300568