Study on mechanical properties of NbC reinforced Nb4AlC3 composites prepared by in situ hot-pressing sintering

Bo Zhang, Jian Yang, Lei Yu, Li Mei Pan, Tai Qiu, Chun Feng Hu

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Abstract

Fully dense NbC reinforced Nb4AlC3 composites were fabricated by reaction in situ hot-pressing sintering at 1700°C using Nb, Al, and C powders as raw materials. The phase composition and microstructure of the materials were characterized by XRD, SEM and EDS analysis. Effects of NbC content on the phases, sintering properties, microstructure, and mechanical properties of the materials were investigated. The results indicate that the in situ incorporation of NbC promotes the sintering of the materials and show significant strengthening and toughening effect. As the NbC content increasing from 0 to 15vol%, both bending strength and fracture toughness increase and then decrease. The 8vol% NbC/Nb4AlC3 composite shows the highest strength of 494 MPa, and toughness of 8.4 MPa·m1/2. The Vickers hardness increases from 2.6 GPa to 4.4 GPa.

Original languageEnglish
Pages (from-to)1144-1148+1161
JournalRengong Jingti Xuebao/Journal of Synthetic Crystals
Volume43
Issue number5
StatePublished - May 2014

Keywords

  • Hot pressing sintering
  • Mechanical property
  • Reaction in-situ

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