TY - JOUR
T1 - Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole
AU - Zhu, Dunru
AU - Zhu, Xiaolei
AU - Xu, Li
AU - Shao, Sichang
AU - Raj, S. Shanmuga Sundara
AU - Fun, Hoong Kun
AU - You, Xiaozeng
PY - 2000/6
Y1 - 2000/6
N2 - The 4-(p-methoxyphenyl)-3,5-bis(4-pyridyl)-1,2,4-triazole has been synthesized and its crystal structure has been determined by X-ray diffraction methods. It crystallizes in the monoclinic space group P21/n, with a = 12.5832(6) Å, b = 7.0512(5) Å, c = 18.4669(12) Å, β = 96.826(1)°, and Dcalc = 1.345 g cm-1 for Z = 4. In the structure, two pyridyl rings, phenyl ring, and triazole ring do not share a common plane. The most favored orientation of the pyridyl rings in the crystal is that their planes are inclined toward opposite directions with respect to the triazole ring.
AB - The 4-(p-methoxyphenyl)-3,5-bis(4-pyridyl)-1,2,4-triazole has been synthesized and its crystal structure has been determined by X-ray diffraction methods. It crystallizes in the monoclinic space group P21/n, with a = 12.5832(6) Å, b = 7.0512(5) Å, c = 18.4669(12) Å, β = 96.826(1)°, and Dcalc = 1.345 g cm-1 for Z = 4. In the structure, two pyridyl rings, phenyl ring, and triazole ring do not share a common plane. The most favored orientation of the pyridyl rings in the crystal is that their planes are inclined toward opposite directions with respect to the triazole ring.
KW - Crystal structure
KW - Triazole
UR - http://www.scopus.com/inward/record.url?scp=0034194949&partnerID=8YFLogxK
U2 - 10.1023/A:1009542208264
DO - 10.1023/A:1009542208264
M3 - 文章
AN - SCOPUS:0034194949
SN - 1074-1542
VL - 30
SP - 429
EP - 432
JO - Journal of Chemical Crystallography
JF - Journal of Chemical Crystallography
IS - 6
ER -