Ultraviolet-initiated synthesis and characterization of anionic polyacrylamide

Jiang Ya Ma; Huai Li Zheng; Wei Lu; Fang Ying Ji; Li Wei Liu; Jun Ren Zhu; Yong Jun Sun

doi:10.3964/j.issn.1000-0593(2012)12-3385-05

Ultraviolet-initiated synthesis and characterization of anionic polyacrylamide

Jiang Ya Ma, Huai Li Zheng, Wei Lu, Fang Ying Ji, Li Wei Liu, Jun Ren Zhu, Yong Jun Sun

Chongqing University

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

APAM was prepared under the action of composite initiator and UV irradiation, using acryl amide (AM), 2-acrylamido-2- methyl propane sulfonic acid (AMPS) and acrylic acid(AA) as raw materials. The paper studied the effect of proportion between monomers, monomer ratio, initiator concentration and other factors on intrinsic viscosity of the polymer, and optimized preparation conditions. The chemical structure and thermal stability of APAM were characterized by UV, FTIR, SEM and DTA-TGA respectively. The results showed that the APAM with the intrinsic viscosity 1.6×10³ mL·g^-1 can prepared when the proportion between monomers was 70:10:10, the monomer ratio was 40%, initiator concentration was 0.20%, pH was 9 and the illu mination time was 60 min.

Original language	English
Pages (from-to)	3385-3389
Number of pages	5
Journal	Guang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysis
Volume	32
Issue number	12
DOIs	https://doi.org/10.3964/j.issn.1000-0593(2012)12-3385-05
State	Published - Dec 2012
Externally published	Yes

Keywords

APAM
Intrinsic viscosity
Spectral analysis
Ultraviolet polymerization

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Cite this

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title = "Ultraviolet-initiated synthesis and characterization of anionic polyacrylamide",

abstract = "APAM was prepared under the action of composite initiator and UV irradiation, using acryl amide (AM), 2-acrylamido-2- methyl propane sulfonic acid (AMPS) and acrylic acid(AA) as raw materials. The paper studied the effect of proportion between monomers, monomer ratio, initiator concentration and other factors on intrinsic viscosity of the polymer, and optimized preparation conditions. The chemical structure and thermal stability of APAM were characterized by UV, FTIR, SEM and DTA-TGA respectively. The results showed that the APAM with the intrinsic viscosity 1.6×103 mL·g-1 can prepared when the proportion between monomers was 70:10:10, the monomer ratio was 40%, initiator concentration was 0.20%, pH was 9 and the illu mination time was 60 min.",

keywords = "APAM, Intrinsic viscosity, Spectral analysis, Ultraviolet polymerization",

author = "Ma, {Jiang Ya} and Zheng, {Huai Li} and Wei Lu and Ji, {Fang Ying} and Liu, {Li Wei} and Zhu, {Jun Ren} and Sun, {Yong Jun}",

year = "2012",

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doi = "10.3964/j.issn.1000-0593(2012)12-3385-05",

language = "英语",

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T1 - Ultraviolet-initiated synthesis and characterization of anionic polyacrylamide

AU - Ma, Jiang Ya

AU - Zheng, Huai Li

AU - Lu, Wei

AU - Ji, Fang Ying

AU - Liu, Li Wei

AU - Zhu, Jun Ren

AU - Sun, Yong Jun

PY - 2012/12

Y1 - 2012/12

N2 - APAM was prepared under the action of composite initiator and UV irradiation, using acryl amide (AM), 2-acrylamido-2- methyl propane sulfonic acid (AMPS) and acrylic acid(AA) as raw materials. The paper studied the effect of proportion between monomers, monomer ratio, initiator concentration and other factors on intrinsic viscosity of the polymer, and optimized preparation conditions. The chemical structure and thermal stability of APAM were characterized by UV, FTIR, SEM and DTA-TGA respectively. The results showed that the APAM with the intrinsic viscosity 1.6×103 mL·g-1 can prepared when the proportion between monomers was 70:10:10, the monomer ratio was 40%, initiator concentration was 0.20%, pH was 9 and the illu mination time was 60 min.

AB - APAM was prepared under the action of composite initiator and UV irradiation, using acryl amide (AM), 2-acrylamido-2- methyl propane sulfonic acid (AMPS) and acrylic acid(AA) as raw materials. The paper studied the effect of proportion between monomers, monomer ratio, initiator concentration and other factors on intrinsic viscosity of the polymer, and optimized preparation conditions. The chemical structure and thermal stability of APAM were characterized by UV, FTIR, SEM and DTA-TGA respectively. The results showed that the APAM with the intrinsic viscosity 1.6×103 mL·g-1 can prepared when the proportion between monomers was 70:10:10, the monomer ratio was 40%, initiator concentration was 0.20%, pH was 9 and the illu mination time was 60 min.

KW - APAM

KW - Intrinsic viscosity

KW - Spectral analysis

KW - Ultraviolet polymerization

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DO - 10.3964/j.issn.1000-0593(2012)12-3385-05

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SN - 1000-0593

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JO - Guang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysis

JF - Guang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysis

IS - 12

ER -

Ultraviolet-initiated synthesis and characterization of anionic polyacrylamide

Abstract

Keywords

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