TY - JOUR
T1 - 2-(1,5-Diphenyl-1H-pyrazol-3-yl-oxy)-1-(2-sulfanyl-idene-1, 3-thia-zolidin-3-yl)-ethanone
AU - Li, Yi
AU - Liu, Yuan Yuan
AU - Xiong, Xiao Hui
AU - Wei, Ping
PY - 2012/8
Y1 - 2012/8
N2 - The title compound, C20H17N3O2S2, was synthesized by the reaction of 2-(1,5-diphenyl-1H-pyrazol-3-yl-oxy)acetic acid and thia-zolidine-2-thione. The C-linked benzene ring, N-linked benzene ring and thia-zolidine-2-thione ring are twisted 31.33 (2), 62.87 (1) and 82.71 (2)°, respectively, from the plane of the bridging 1H-pyrazole ring. The phenyl rings are oriented at a dihedral angle of 72.16 (2)°.
AB - The title compound, C20H17N3O2S2, was synthesized by the reaction of 2-(1,5-diphenyl-1H-pyrazol-3-yl-oxy)acetic acid and thia-zolidine-2-thione. The C-linked benzene ring, N-linked benzene ring and thia-zolidine-2-thione ring are twisted 31.33 (2), 62.87 (1) and 82.71 (2)°, respectively, from the plane of the bridging 1H-pyrazole ring. The phenyl rings are oriented at a dihedral angle of 72.16 (2)°.
KW - R factor = 0.068
KW - T = 293 K
KW - data-to-parameter ratio = 13.9
KW - mean σ(C-C) = 0.007 Å
KW - single-crystal X-ray study
KW - wR factor = 0.149
UR - http://www.scopus.com/inward/record.url?scp=84864697607&partnerID=8YFLogxK
U2 - 10.1107/S1600536812029959
DO - 10.1107/S1600536812029959
M3 - 文章
AN - SCOPUS:84864697607
SN - 1600-5368
VL - 68
SP - o2419
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 8
ER -