A simple oxazolidine linker for solid-phase synthesis of peptide aldehydes

Wu Kang, Weiguo Wang, Xiaoxia Zhi, Bo Zhang, Ping Wei, Hongyan Xu

科研成果: 期刊稿件文章同行评审

10 引用 (Scopus)

摘要

A very simple and cheap linker has been used for solid-phase synthesis of peptide aldehydes. Protected amino acid aldehydes are immobilized on 2-Cl(trt) resin as oxazolidine formation via diethanolamine. After classical Fmoc SPPS, treatment of the resin with AcOH/DCM/H 2O (8:1:1) affords peptide aldehydes in high yield and purity.

源语言英语
页(从-至)1187-1188
页数2
期刊Bioorganic and Medicinal Chemistry Letters
22
2
DOI
出版状态已出版 - 15 1月 2012

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