Preparation and Characterization of TiO2-pillared Layered HNb3O8

Xian Ji Guo, Wen Hua Hou, Yan Kong, Wei Ping Ding, Yi Ning Fan, Tian Yang Yao, Qi Jie Yan, Yi Chen

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2 引用 (Scopus)

摘要

Oligomeric titanium(IV) cation ([Ti(OH)x(H2O) y]z+)-intercalated niobate was prepared through a stepwise ion-exchange route, in which n-decylamine was employed as a preswelling agent and titanium isopropoxide as titanium source. Titania-pillared layered niobic acid was then obtained by calcining oligomeric titanium(IV) cation-intercalated niobate at 450 °C in air. Characterization of this pillared material indicated that the material had a porous layered structure with an interlayer distance of 1.38 nm and a BET (Brunauer-Emmett-Teller) surface area of 34 m2 · g -1. The layered structure was still retained after the pillared material was heated at 550 °C.

源语言英语
页(从-至)340-343
页数4
期刊Chinese Journal of Chemistry
22
4
DOI
出版状态已出版 - 4月 2004
已对外发布

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