1,5-Bis[(2-methoxyethoxy)methyl]-1,5-naphthyridine-4,8(1H,5H)-dione

Kunyan Wang; Chen Chen; Peng Jiang; Lu Shi; Hong Jun Zhu

doi:10.1107/S1600536811054547

1,5-Bis[(2-methoxyethoxy)methyl]-1,5-naphthyridine-4,8(1H,5H)-dione

Kunyan Wang, Chen Chen, Peng Jiang, Lu Shi, Hong Jun Zhu

School of Chemistry and Moleculai Engineering

Nanjing Tech University

Research output: Contribution to journal › Article › peer-review

Abstract

The complete molecule of the title compound, C ₁₆H ₂₂N ₂O ₆, is generated by crystallographic inversion symmetry. The conformation of the N - C - O - C fragment of the side chain is approximately gauche [torsion angle = -74.84 (17)°]. In the crystal, weak C - H⋯O interactions link the molecules.

Original language	English
Pages (from-to)	o280
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	68
Issue number	2
DOIs	https://doi.org/10.1107/S1600536811054547
State	Published - Feb 2012

Keywords

R factor = 0.045
T = 293 K
data-to-parameter ratio = 14.1
mean σ(C-C) = 0.002 Å
single-crystal X-ray study
wR factor = 0.140

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title = "1,5-Bis[(2-methoxyethoxy)methyl]-1,5-naphthyridine-4,8(1H,5H)-dione",

abstract = "The complete molecule of the title compound, C 16H 22N 2O 6, is generated by crystallographic inversion symmetry. The conformation of the N - C - O - C fragment of the side chain is approximately gauche [torsion angle = -74.84 (17)°]. In the crystal, weak C - H⋯O interactions link the molecules.",

keywords = "R factor = 0.045, T = 293 K, data-to-parameter ratio = 14.1, mean σ(C-C) = 0.002 {\AA}, single-crystal X-ray study, wR factor = 0.140",

author = "Kunyan Wang and Chen Chen and Peng Jiang and Lu Shi and Zhu, {Hong Jun}",

year = "2012",

month = feb,

doi = "10.1107/S1600536811054547",

language = "英语",

volume = "68",

pages = "o280",

journal = "Acta Crystallographica Section E: Structure Reports Online",

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TY - JOUR

T1 - 1,5-Bis[(2-methoxyethoxy)methyl]-1,5-naphthyridine-4,8(1H,5H)-dione

AU - Wang, Kunyan

AU - Chen, Chen

AU - Jiang, Peng

AU - Shi, Lu

AU - Zhu, Hong Jun

PY - 2012/2

Y1 - 2012/2

N2 - The complete molecule of the title compound, C 16H 22N 2O 6, is generated by crystallographic inversion symmetry. The conformation of the N - C - O - C fragment of the side chain is approximately gauche [torsion angle = -74.84 (17)°]. In the crystal, weak C - H⋯O interactions link the molecules.

AB - The complete molecule of the title compound, C 16H 22N 2O 6, is generated by crystallographic inversion symmetry. The conformation of the N - C - O - C fragment of the side chain is approximately gauche [torsion angle = -74.84 (17)°]. In the crystal, weak C - H⋯O interactions link the molecules.

KW - R factor = 0.045

KW - T = 293 K

KW - data-to-parameter ratio = 14.1

KW - mean σ(C-C) = 0.002 Å

KW - single-crystal X-ray study

KW - wR factor = 0.140

UR - http://www.scopus.com/inward/record.url?scp=84863027139&partnerID=8YFLogxK

U2 - 10.1107/S1600536811054547

DO - 10.1107/S1600536811054547

M3 - 文章

AN - SCOPUS:84863027139

SN - 1600-5368

VL - 68

SP - o280

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 2

ER -

1,5-Bis[(2-methoxyethoxy)methyl]-1,5-naphthyridine-4,8(1H,5H)-dione

Abstract

Keywords

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