Preparation of SiC nanoparticles coated by ZnC2O4

Sheng Cui; Xiaodong Shen; Su Xiao; Zhiqiang Gao; Benlan Lin

Preparation of SiC nanoparticles coated by ZnC₂O₄

Sheng Cui, Xiaodong Shen, Su Xiao, Zhiqiang Gao, Benlan Lin

College of Materials Science and Engineering

Nanjing Tech University

Research output: Contribution to journal › Article › peer-review

Abstract

Sol-gel method was used to produce SiC particles coated with dihydrated zinc oxalate. The effect of main salt concentration and aging time on the coating was investigated. Dihydrated zinc acetate and oxalic acid are put into ethanol and heated to make ethanol solution of dihydrated zinc acetate and ethanol solution of oxalic acid respectively, with their mol ratio of 1:1.2 and Zn²⁺ concentration of 1.5mol·L^-1. SiC particles dispersed by ultrasonic for 5min and ethanol solution of oxalic acid are put into ethanol solution of dihydrated zinc acetate to make mixed solution. The mixed solution is stirred at high speed in a water-hath at 75°C and then gelatin is formed. SiC particles coated with zinc oxalate are obtained by aging for 4h and dryness. It is shown by means of HRTEM and EDS that SiC particles are dispersed in the gel of dihydrated zinc oxalate.

Original language	English
Pages (from-to)	86-90
Number of pages	5
Journal	Fenmo Yejin Jishu/Powder Metallurgy Technology
Volume	27
Issue number	2
State	Published - Apr 2009

Keywords

Characterization
SiC nanoparticles
Sol-gel method
ZnCO

Cite this

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title = "Preparation of SiC nanoparticles coated by ZnC2O4",

abstract = "Sol-gel method was used to produce SiC particles coated with dihydrated zinc oxalate. The effect of main salt concentration and aging time on the coating was investigated. Dihydrated zinc acetate and oxalic acid are put into ethanol and heated to make ethanol solution of dihydrated zinc acetate and ethanol solution of oxalic acid respectively, with their mol ratio of 1:1.2 and Zn2+ concentration of 1.5mol·L-1. SiC particles dispersed by ultrasonic for 5min and ethanol solution of oxalic acid are put into ethanol solution of dihydrated zinc acetate to make mixed solution. The mixed solution is stirred at high speed in a water-hath at 75°C and then gelatin is formed. SiC particles coated with zinc oxalate are obtained by aging for 4h and dryness. It is shown by means of HRTEM and EDS that SiC particles are dispersed in the gel of dihydrated zinc oxalate.",

keywords = "Characterization, SiC nanoparticles, Sol-gel method, ZnCO",

author = "Sheng Cui and Xiaodong Shen and Su Xiao and Zhiqiang Gao and Benlan Lin",

year = "2009",

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language = "英语",

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journal = "Fenmo Yejin Jishu/Powder Metallurgy Technology",

issn = "1001-3784",

publisher = "University of Science and Technology Beijing",

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TY - JOUR

T1 - Preparation of SiC nanoparticles coated by ZnC2O4

AU - Cui, Sheng

AU - Shen, Xiaodong

AU - Xiao, Su

AU - Gao, Zhiqiang

AU - Lin, Benlan

PY - 2009/4

Y1 - 2009/4

N2 - Sol-gel method was used to produce SiC particles coated with dihydrated zinc oxalate. The effect of main salt concentration and aging time on the coating was investigated. Dihydrated zinc acetate and oxalic acid are put into ethanol and heated to make ethanol solution of dihydrated zinc acetate and ethanol solution of oxalic acid respectively, with their mol ratio of 1:1.2 and Zn2+ concentration of 1.5mol·L-1. SiC particles dispersed by ultrasonic for 5min and ethanol solution of oxalic acid are put into ethanol solution of dihydrated zinc acetate to make mixed solution. The mixed solution is stirred at high speed in a water-hath at 75°C and then gelatin is formed. SiC particles coated with zinc oxalate are obtained by aging for 4h and dryness. It is shown by means of HRTEM and EDS that SiC particles are dispersed in the gel of dihydrated zinc oxalate.

AB - Sol-gel method was used to produce SiC particles coated with dihydrated zinc oxalate. The effect of main salt concentration and aging time on the coating was investigated. Dihydrated zinc acetate and oxalic acid are put into ethanol and heated to make ethanol solution of dihydrated zinc acetate and ethanol solution of oxalic acid respectively, with their mol ratio of 1:1.2 and Zn2+ concentration of 1.5mol·L-1. SiC particles dispersed by ultrasonic for 5min and ethanol solution of oxalic acid are put into ethanol solution of dihydrated zinc acetate to make mixed solution. The mixed solution is stirred at high speed in a water-hath at 75°C and then gelatin is formed. SiC particles coated with zinc oxalate are obtained by aging for 4h and dryness. It is shown by means of HRTEM and EDS that SiC particles are dispersed in the gel of dihydrated zinc oxalate.

KW - Characterization

KW - SiC nanoparticles

KW - Sol-gel method

KW - ZnCO

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M3 - 文章

AN - SCOPUS:66149169769

SN - 1001-3784

VL - 27

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JO - Fenmo Yejin Jishu/Powder Metallurgy Technology

JF - Fenmo Yejin Jishu/Powder Metallurgy Technology

IS - 2

ER -

Preparation of SiC nanoparticles coated by ZnC₂O₄

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Keywords

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