TY - JOUR
T1 - Synthesis of N-(5-aryl-1,3,4-thiadiazol-2-yl)-2-(3-oxo-1,2-benzothiazol- 2(3H)-yl)acetamide derivatives promoted by carbodiimide condensation
AU - Yu, Peng
AU - Hu, Jun
AU - Wan, Rong
AU - Li, Xi
AU - Zheng, Shanlong
AU - Xu, Yanhua
PY - 2014/6
Y1 - 2014/6
N2 - Novel N-(5-aryl-1,3,4-thiadiazol-2-yl)-2-(3-oxo-1,2-benzothiazol-2(3H)-yl) acetamide derivatives were prepared by 1-(3-dimethylaminopropyl)-3- ethylcarbodiimide hydrochloride and N-hydroxybenzotrizole condensation catalysis in a convenient and fast method. These compounds were identified by IR, 1H NMR and elemental analyses and the intermediate compound 5-(2-chlorophenyl)-1,3,4-thiadiazol-2-amine was confirmed by single-crystal X-ray diffraction.
AB - Novel N-(5-aryl-1,3,4-thiadiazol-2-yl)-2-(3-oxo-1,2-benzothiazol-2(3H)-yl) acetamide derivatives were prepared by 1-(3-dimethylaminopropyl)-3- ethylcarbodiimide hydrochloride and N-hydroxybenzotrizole condensation catalysis in a convenient and fast method. These compounds were identified by IR, 1H NMR and elemental analyses and the intermediate compound 5-(2-chlorophenyl)-1,3,4-thiadiazol-2-amine was confirmed by single-crystal X-ray diffraction.
KW - 1-2-benzisothiazolin-3-one
KW - 1-3-4-thiadiazole
KW - Acetamide synthesis
UR - http://www.scopus.com/inward/record.url?scp=84903317573&partnerID=8YFLogxK
U2 - 10.3184/174751914X13990224465880
DO - 10.3184/174751914X13990224465880
M3 - 文章
AN - SCOPUS:84903317573
SN - 1747-5198
VL - 38
SP - 347
EP - 350
JO - Journal of Chemical Research
JF - Journal of Chemical Research
IS - 6
ER -