A facile template-free route to synthesize porous ZnO nanosheets with high surface area

Xiulan Hua; Xiaodong Shen; Rong Huang; Yoshitake Masuda; Tatsuki Ohji; Kazumi Kato

doi:10.1016/j.jallcom.2013.06.089

A facile template-free route to synthesize porous ZnO nanosheets with high surface area

Xiulan Hua, Xiaodong Shen, Rong Huang, Yoshitake Masuda, Tatsuki Ohji, Kazumi Kato

材料科学与工程学院

科研成果: 期刊稿件 › 文章 › 同行评审

19 引用（Scopus）

摘要

Microporous and mesoporous ZnO nanosheets were successfully synthesized by a lowerature chemical bath deposition and subsequently thermal decomposition at 250 °C without any templates. Nanosheet-shaped zinc hydroxide nitrate (Zn₃(OH)₄(NO₃)₂) was formed as the precursors at 90 C for 6 days by chemical bath deposition in a close system. Microporous and mesoporous ZnO nanosheets were obtained from the removing of OH and NO3 groups from zinc hydroxide nitrate (Zn₃(OH) ₄(NO₃)₂) nanosheet- shaped precursors. The pore sizes were distributed in the region of ∼1.3-25 nm with a center at ∼2.4 nm. Such porous and nanosheets structure gave a highest specific surface area of 283.8 m²/g.

源语言	英语
页（从-至）	373-376
页数	4
期刊	Journal of Alloys and Compounds
卷	580
DOI	https://doi.org/10.1016/j.jallcom.2013.06.089
出版状态	已出版 - 2013

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10.1016/j.jallcom.2013.06.089

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abstract = "Microporous and mesoporous ZnO nanosheets were successfully synthesized by a lowerature chemical bath deposition and subsequently thermal decomposition at 250 °C without any templates. Nanosheet-shaped zinc hydroxide nitrate (Zn3(OH)4(NO3)2) was formed as the precursors at 90 C for 6 days by chemical bath deposition in a close system. Microporous and mesoporous ZnO nanosheets were obtained from the removing of OH and NO3 groups from zinc hydroxide nitrate (Zn3(OH) 4(NO3)2) nanosheet- shaped precursors. The pore sizes were distributed in the region of ∼1.3-25 nm with a center at ∼2.4 nm. Such porous and nanosheets structure gave a highest specific surface area of 283.8 m2/g.",

keywords = "Chemical deposition, Nanosheets, Porous materials, ZnO",

author = "Xiulan Hua and Xiaodong Shen and Rong Huang and Yoshitake Masuda and Tatsuki Ohji and Kazumi Kato",

year = "2013",

doi = "10.1016/j.jallcom.2013.06.089",

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T1 - A facile template-free route to synthesize porous ZnO nanosheets with high surface area

AU - Hua, Xiulan

AU - Shen, Xiaodong

AU - Huang, Rong

AU - Masuda, Yoshitake

AU - Ohji, Tatsuki

AU - Kato, Kazumi

PY - 2013

Y1 - 2013

N2 - Microporous and mesoporous ZnO nanosheets were successfully synthesized by a lowerature chemical bath deposition and subsequently thermal decomposition at 250 °C without any templates. Nanosheet-shaped zinc hydroxide nitrate (Zn3(OH)4(NO3)2) was formed as the precursors at 90 C for 6 days by chemical bath deposition in a close system. Microporous and mesoporous ZnO nanosheets were obtained from the removing of OH and NO3 groups from zinc hydroxide nitrate (Zn3(OH) 4(NO3)2) nanosheet- shaped precursors. The pore sizes were distributed in the region of ∼1.3-25 nm with a center at ∼2.4 nm. Such porous and nanosheets structure gave a highest specific surface area of 283.8 m2/g.

AB - Microporous and mesoporous ZnO nanosheets were successfully synthesized by a lowerature chemical bath deposition and subsequently thermal decomposition at 250 °C without any templates. Nanosheet-shaped zinc hydroxide nitrate (Zn3(OH)4(NO3)2) was formed as the precursors at 90 C for 6 days by chemical bath deposition in a close system. Microporous and mesoporous ZnO nanosheets were obtained from the removing of OH and NO3 groups from zinc hydroxide nitrate (Zn3(OH) 4(NO3)2) nanosheet- shaped precursors. The pore sizes were distributed in the region of ∼1.3-25 nm with a center at ∼2.4 nm. Such porous and nanosheets structure gave a highest specific surface area of 283.8 m2/g.

KW - Chemical deposition

KW - Nanosheets

KW - Porous materials

KW - ZnO

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U2 - 10.1016/j.jallcom.2013.06.089

DO - 10.1016/j.jallcom.2013.06.089

M3 - 文章

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SN - 0925-8388

VL - 580

SP - 373

EP - 376

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

ER -

A facile template-free route to synthesize porous ZnO nanosheets with high surface area

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