Crystal structure and characterization of 2-N-(2-hydroxy-benzylidene) furanmethanoamine nickel(II) complex

Jun Wang; Hong Xu; Hua Zhou; Ping Wei

Crystal structure and characterization of 2-N-(2-hydroxy-benzylidene) furanmethanoamine nickel(II) complex

Jun Wang, Hong Xu, Hua Zhou, Ping Wei

生物与制药工程学院

科研成果: 期刊稿件 › 文章 › 同行评审

10 引用（Scopus）

摘要

The Ni(II) complex with ligand 2-N-(2-hydroxy-benzylidene) furanmethanoamine has been synthesized and characterized by elemental analysis, IR and single-crystal X-ray diffraction. It crystallizes in the monoclinic system, space group C2/c with a = 2.0280(4), b = 0.57700(12), c = 1.7340(4) nm, β = 94.74(3)°, Z = 4, D_c = 1.508 g/cm³, the final R = 0.0434 and wR = 0.1112 for 1843 observed reflections with I > 2σ(I). X-ray analysis revealed that the Ni(II) ion is coordinated by two nitrogen atoms of Schiff base and two oxygen atoms of salicylaldehyde in the equatorial plane, and the coordination geometry can be described as a square.

源语言	英语
页（从-至）	909-912
页数	4
期刊	Jiegou Huaxue
卷	24
期	8
出版状态	已出版 - 2005

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title = "Crystal structure and characterization of 2-N-(2-hydroxy-benzylidene) furanmethanoamine nickel(II) complex",

abstract = "The Ni(II) complex with ligand 2-N-(2-hydroxy-benzylidene) furanmethanoamine has been synthesized and characterized by elemental analysis, IR and single-crystal X-ray diffraction. It crystallizes in the monoclinic system, space group C2/c with a = 2.0280(4), b = 0.57700(12), c = 1.7340(4) nm, β = 94.74(3)°, Z = 4, Dc = 1.508 g/cm3, the final R = 0.0434 and wR = 0.1112 for 1843 observed reflections with I > 2σ(I). X-ray analysis revealed that the Ni(II) ion is coordinated by two nitrogen atoms of Schiff base and two oxygen atoms of salicylaldehyde in the equatorial plane, and the coordination geometry can be described as a square.",

keywords = "Crystal structure, Furfuryl amine, Nickel(II) complex, Salicylaldehyde, Schiff base",

author = "Jun Wang and Hong Xu and Hua Zhou and Ping Wei",

year = "2005",

language = "英语",

volume = "24",

pages = "909--912",

journal = "Jiegou Huaxue",

issn = "0254-5861",

publisher = "Fujian Institute of Research of the Structure of Matter",

number = "8",

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TY - JOUR

T1 - Crystal structure and characterization of 2-N-(2-hydroxy-benzylidene) furanmethanoamine nickel(II) complex

AU - Wang, Jun

AU - Xu, Hong

AU - Zhou, Hua

AU - Wei, Ping

PY - 2005

Y1 - 2005

N2 - The Ni(II) complex with ligand 2-N-(2-hydroxy-benzylidene) furanmethanoamine has been synthesized and characterized by elemental analysis, IR and single-crystal X-ray diffraction. It crystallizes in the monoclinic system, space group C2/c with a = 2.0280(4), b = 0.57700(12), c = 1.7340(4) nm, β = 94.74(3)°, Z = 4, Dc = 1.508 g/cm3, the final R = 0.0434 and wR = 0.1112 for 1843 observed reflections with I > 2σ(I). X-ray analysis revealed that the Ni(II) ion is coordinated by two nitrogen atoms of Schiff base and two oxygen atoms of salicylaldehyde in the equatorial plane, and the coordination geometry can be described as a square.

AB - The Ni(II) complex with ligand 2-N-(2-hydroxy-benzylidene) furanmethanoamine has been synthesized and characterized by elemental analysis, IR and single-crystal X-ray diffraction. It crystallizes in the monoclinic system, space group C2/c with a = 2.0280(4), b = 0.57700(12), c = 1.7340(4) nm, β = 94.74(3)°, Z = 4, Dc = 1.508 g/cm3, the final R = 0.0434 and wR = 0.1112 for 1843 observed reflections with I > 2σ(I). X-ray analysis revealed that the Ni(II) ion is coordinated by two nitrogen atoms of Schiff base and two oxygen atoms of salicylaldehyde in the equatorial plane, and the coordination geometry can be described as a square.

KW - Crystal structure

KW - Furfuryl amine

KW - Nickel(II) complex

KW - Salicylaldehyde

KW - Schiff base

UR - http://www.scopus.com/inward/record.url?scp=24344475657&partnerID=8YFLogxK

M3 - 文章

AN - SCOPUS:24344475657

SN - 0254-5861

VL - 24

SP - 909

EP - 912

JO - Jiegou Huaxue

JF - Jiegou Huaxue

IS - 8

ER -

Crystal structure and characterization of 2-N-(2-hydroxy-benzylidene) furanmethanoamine nickel(II) complex

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