Abstract
C4H3O5Na(0.5H2O) was prepared by the reaction of H2O2 and maleic anhydride. The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to monoclinic, space group C2/c with a = 21.132(3), b = 8.646(2), c = 6.196(1) Å, β= 90.67(1)°, V = 1132.0(4) Å3, Mr = 163.06, Dc = 1.914 g/cm3, Z = 8, F(000) = 664, μ = 0.243 mm-1, the final R = 0.0354 and wR = 0.1151. X-ray analysis reveals that there exists a stable symmetrical structure in the complex, and a network structure is formed via intermolecular hydrogen bonds.
| Original language | English |
|---|---|
| Pages (from-to) | 259-262 |
| Number of pages | 4 |
| Journal | Jiegou Huaxue |
| Volume | 24 |
| Issue number | 3 |
| State | Published - 2005 |
Keywords
- Crystal structure
- Preparation
- Sodium hydrogen epoxysuccinate