Preparation and crystal structure of sodium hydrogen epoxysuccinate

He Min Li; Hong Jun Zhu; Hua Jin; Ji Ma; Jin Tang Wang

Preparation and crystal structure of sodium hydrogen epoxysuccinate

He Min Li, Hong Jun Zhu, Hua Jin, Ji Ma, Jin Tang Wang

化学与分子工程学院

Nanjing Tech University

科研成果: 期刊稿件 › 文章 › 同行评审

3 引用（Scopus）

摘要

C₄H₃O₅Na(0.5H₂O) was prepared by the reaction of H₂O₂ and maleic anhydride. The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to monoclinic, space group C2/c with a = 21.132(3), b = 8.646(2), c = 6.196(1) Å, β= 90.67(1)°, V = 1132.0(4) Å³, M_r = 163.06, D_c = 1.914 g/cm³, Z = 8, F(000) = 664, μ = 0.243 mm^-1, the final R = 0.0354 and wR = 0.1151. X-ray analysis reveals that there exists a stable symmetrical structure in the complex, and a network structure is formed via intermolecular hydrogen bonds.

源语言	英语
页（从-至）	259-262
页数	4
期刊	Jiegou Huaxue
卷	24
期	3
出版状态	已出版 - 2005

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title = "Preparation and crystal structure of sodium hydrogen epoxysuccinate",

abstract = "C4H3O5Na(0.5H2O) was prepared by the reaction of H2O2 and maleic anhydride. The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to monoclinic, space group C2/c with a = 21.132(3), b = 8.646(2), c = 6.196(1) {\AA}, β= 90.67(1)°, V = 1132.0(4) {\AA}3, Mr = 163.06, Dc = 1.914 g/cm3, Z = 8, F(000) = 664, μ = 0.243 mm-1, the final R = 0.0354 and wR = 0.1151. X-ray analysis reveals that there exists a stable symmetrical structure in the complex, and a network structure is formed via intermolecular hydrogen bonds.",

keywords = "Crystal structure, Preparation, Sodium hydrogen epoxysuccinate",

author = "Li, {He Min} and Zhu, {Hong Jun} and Hua Jin and Ji Ma and Wang, {Jin Tang}",

year = "2005",

language = "英语",

volume = "24",

pages = "259--262",

journal = "Jiegou Huaxue",

issn = "0254-5861",

publisher = "Fujian Institute of Research of the Structure of Matter",

number = "3",

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TY - JOUR

T1 - Preparation and crystal structure of sodium hydrogen epoxysuccinate

AU - Li, He Min

AU - Zhu, Hong Jun

AU - Jin, Hua

AU - Ma, Ji

AU - Wang, Jin Tang

PY - 2005

Y1 - 2005

N2 - C4H3O5Na(0.5H2O) was prepared by the reaction of H2O2 and maleic anhydride. The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to monoclinic, space group C2/c with a = 21.132(3), b = 8.646(2), c = 6.196(1) Å, β= 90.67(1)°, V = 1132.0(4) Å3, Mr = 163.06, Dc = 1.914 g/cm3, Z = 8, F(000) = 664, μ = 0.243 mm-1, the final R = 0.0354 and wR = 0.1151. X-ray analysis reveals that there exists a stable symmetrical structure in the complex, and a network structure is formed via intermolecular hydrogen bonds.

AB - C4H3O5Na(0.5H2O) was prepared by the reaction of H2O2 and maleic anhydride. The product was characterized by elemental analysis and IR measurement. The crystal structure was determined by single-crystal diffraction analysis. The crystal belongs to monoclinic, space group C2/c with a = 21.132(3), b = 8.646(2), c = 6.196(1) Å, β= 90.67(1)°, V = 1132.0(4) Å3, Mr = 163.06, Dc = 1.914 g/cm3, Z = 8, F(000) = 664, μ = 0.243 mm-1, the final R = 0.0354 and wR = 0.1151. X-ray analysis reveals that there exists a stable symmetrical structure in the complex, and a network structure is formed via intermolecular hydrogen bonds.

KW - Crystal structure

KW - Preparation

KW - Sodium hydrogen epoxysuccinate

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M3 - 文章

AN - SCOPUS:16344384881

SN - 0254-5861

VL - 24

SP - 259

EP - 262

JO - Jiegou Huaxue

JF - Jiegou Huaxue

IS - 3

ER -

Preparation and crystal structure of sodium hydrogen epoxysuccinate

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