Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

Yong Fei Zhou; Shi Pei Zhang; Zhe Feng; Xuan Shen; Dun Ru Zhu

doi:10.1002/jhet.2880

Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

Yong Fei Zhou, Shi Pei Zhang, Zhe Feng, Xuan Shen, Dun Ru Zhu

College of Chemical Engineering

Nanjing Tech University

Research output: Contribution to journal › Article › peer-review

6 Scopus citations

Abstract

Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L¹: R = OCH₃; L²: R = CH₃; L³: R = H; L⁴: R = Br; L⁵: R = Cl; L⁶: R = F) were successfully synthesized. Yield of L^1–6 is in the range from 61 to 76%. The compounds L^1–6 were characterized by UV–vis, FTIR, ¹H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L^1–5 were determined by single crystal X-ray crystallography.

Original language	English
Pages (from-to)	2773-2780
Number of pages	8
Journal	Journal of Heterocyclic Chemistry
Volume	54
Issue number	5
DOIs	https://doi.org/10.1002/jhet.2880
State	Published - Sep 2017

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title = "Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles",

abstract = "Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.",

author = "Zhou, {Yong Fei} and Zhang, {Shi Pei} and Zhe Feng and Xuan Shen and Zhu, {Dun Ru}",

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T1 - Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

AU - Zhou, Yong Fei

AU - Zhang, Shi Pei

AU - Feng, Zhe

AU - Shen, Xuan

AU - Zhu, Dun Ru

PY - 2017/9

Y1 - 2017/9

N2 - Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.

AB - Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.

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DO - 10.1002/jhet.2880

M3 - 文章

AN - SCOPUS:85017564225

SN - 0022-152X

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JO - Journal of Heterocyclic Chemistry

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ER -

Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

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