Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

Yong Fei Zhou; Shi Pei Zhang; Zhe Feng; Xuan Shen; Dun Ru Zhu

doi:10.1002/jhet.2880

Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

Yong Fei Zhou, Shi Pei Zhang, Zhe Feng, Xuan Shen, Dun Ru Zhu

化工学院

Nanjing Tech University

科研成果: 期刊稿件 › 文章 › 同行评审

6 引用（Scopus）

摘要

Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L¹: R = OCH₃; L²: R = CH₃; L³: R = H; L⁴: R = Br; L⁵: R = Cl; L⁶: R = F) were successfully synthesized. Yield of L^1–6 is in the range from 61 to 76%. The compounds L^1–6 were characterized by UV–vis, FTIR, ¹H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L^1–5 were determined by single crystal X-ray crystallography.

源语言	英语
页（从-至）	2773-2780
页数	8
期刊	Journal of Heterocyclic Chemistry
卷	54
期	5
DOI	https://doi.org/10.1002/jhet.2880
出版状态	已出版 - 9月 2017

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title = "Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles",

abstract = "Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.",

author = "Zhou, {Yong Fei} and Zhang, {Shi Pei} and Zhe Feng and Xuan Shen and Zhu, {Dun Ru}",

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T1 - Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

AU - Zhou, Yong Fei

AU - Zhang, Shi Pei

AU - Feng, Zhe

AU - Shen, Xuan

AU - Zhu, Dun Ru

PY - 2017/9

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N2 - Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.

AB - Six new benzimidazolyl substituted triaryltriazoles, 3-(2-pyridyl)-4-(p-R-phenyl)-5-(2-benzimidazolyl)-1,2,4-triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H-NMR, ESI-MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X-ray crystallography.

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DO - 10.1002/jhet.2880

M3 - 文章

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SN - 0022-152X

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JO - Journal of Heterocyclic Chemistry

JF - Journal of Heterocyclic Chemistry

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Syntheses, Crystal Structures, and Spectral Characterization of Six Novel Benzimidazolyl Substituted Triaryltriazoles

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